Study on Volatile Oils from Calendula officinalis Prepared by Headspace Liquid Phase Microextraction and Steam Distillation

您当前的位置：

首页 >

文章列表页 >

Study on Volatile Oils from Calendula officinalis Prepared by Headspace Liquid Phase Microextraction and Steam Distillation

更新时间：2023-12-11

- Study on Volatile Oils from Calendula officinalis Prepared by Headspace Liquid Phase Microextraction and Steam Distillation
- Acta Scientiarum Naturalium Universitatis SunYatseni Vol. 49, Issue 1, Pages: 145-148(2010)
- 作者机构：
  
  1. ．中山大学药学院生药学与天然药物化学实验室,广东,广州,510006
  2.  2．南方医科大学南方医院药学部,广东,广州,510515
  3. 3．珠海安和生化科技有限公司芳香技术研发中心,广东,珠海,519040
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Published：2010，
  
  Published Online：25 January 2010，
扫描看全文
Study on Volatile Oils from Calendula officinalis Prepared by Headspace Liquid Phase Microextraction and Steam Distillation. [J]. Acta Scientiarum Naturalium Universitatis SunYatseni 49(1):145-148(2010)
DOI：

Study on Volatile Oils from Calendula officinalis Prepared by Headspace Liquid Phase Microextraction and Steam Distillation. [J]. Acta Scientiarum Naturalium Universitatis SunYatseni 49(1):145-148(2010) DOI：

摘要

采用顶空液相微萃取法（HS-LPME）与水蒸气蒸馏法（SD）分别提取金盏花中的挥发性成分，经GC-MS分析，通过质谱图计算机辅助谱库检索和人工解析相结合、并参考相关文献进行化合物的定性分析，以峰面积归一化法计算各组分的相对含量。HS-LPME法所得挥发油提取物中鉴定出15种化合物，在SD法提取的挥发油中共鉴定出31种化合物，两者共有成分为14个，其中主要成分均为α-杜松醇，τ-依兰油醇，δ-杜松烯，α-依兰油烯，τ-杜松烯等，且相对含量无显著差异，5个化合物的总含量分别占总挥发油的93.43% （HS-LPME法）和87.18%（SD法）。

Abstract

The volatile oils were prepared from Calendula officinalis by headspace liquid phase microextraction (HSLPME) and steam distillation (SD). Their constituents were analyzed and identified by gas chromatographymass spectrometry combined with computer retrieval

and were quantified by calculating the relative contents basing on the peak areas normalization method. The results showed that fifteen components were identified for the volatile oil extracted by HS-LPME

and thirtyone components were identified for that extracted by SD. However

the main components obtained from both methods were found to be quite similar. Among the fourteen mutual components

α-cadinol

τ-Muurolol

τ-cadinene

δ-cadinene

α-muurolene were the main components

occupied 93.43% and 87.18% of the total volatile oils prepared by HS-LPME and SD

respectively. It was also observed that there were no significant differences in the relative contents of these five components between the two methods.

关键词

金盏花挥发油水蒸气蒸馏法顶空液相微萃取法GC-MS

Keywords

Calendula officinalis (Pot Marigold)volatile oilsteam distillationheadspace liquid phase microextractionGC-MS

references

Views

148

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Dynamic change and activity analysis of volatile oil in the flowers of Citri Grandis Exocarpium

Determination of Chemical Compositions of the Volatile Oil fromMicro-milling and Ordinary Pulverization of the Leaves of Celastrus rosthornianus Loes

GC-MS Quantitative Analysis of GasoLine Trace in Fire Debris

Related Author

LIU Ying

PENG Wei

HU Shuangfei

WU Hao

DONG Li

SU Weiwei

GAO Yuqiong

DING Lina

Related Institution

Department of Chemical Engineering， Maoming Polytechnic

Maoming Branch， Guangdong Laboratory for Lingnan Modern Agriculture

School of Life Sciences， Sun Yat-sen University / Guangdong Engineering and Technology Research Center for Quality and Efficacy Re-valuation of Post-marketed TCM / Guangdong Key Laboratory of Plant Resources

．College of Life Science，Guizhou University



Postal code：510275
Tel：020-84112585，84113223 Email：xuebaozr@mail.sysu.edu.cn
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备09064830号-19 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰