Synthesis and MS/NMR Characterization of the Isomers of Di-hydroxylated Fatty Acid

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Synthesis and MS/NMR Characterization of the Isomers of Di-hydroxylated Fatty Acid

更新时间：2023-12-11

- Synthesis and MS/NMR Characterization of the Isomers of Di-hydroxylated Fatty Acid
- Acta Scientiarum Naturalium Universitatis SunYatseni Vol. 50, Issue 5, Pages: 75-78(2011)
- 作者机构：
  
  1. 南方医科大学生物制药系,广东,广州,510515
  2. 2中山大学药学院,广东,广州,510006
  3. 3悉尼大学药学院，NSW,澳大利亚,2006
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Published：2011，
  
  Published Online：25 September 2011，
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Synthesis and MS/NMR Characterization of the Isomers of Di-hydroxylated Fatty Acid. [J]. Acta Scientiarum Naturalium Universitatis SunYatseni 50(5):75-78(2011)
DOI：

Synthesis and MS/NMR Characterization of the Isomers of Di-hydroxylated Fatty Acid. [J]. Acta Scientiarum Naturalium Universitatis SunYatseni 50(5):75-78(2011) DOI：

摘要

以共轭亚油酸甲酯为原料，与SeO

Abstract

Four di-hydroxy derivatives

including methyl ester of erythro-12

13-dihydroxy-10 E octadecenoic acid，erythro-11

12-dihydroxy-9 E octadecenoic acid，erythro-10

11-dihydroxy-12 E octadecenoic acid and erythro-9

10-dihydroxy-11 E octadecenoic acid

were synthesized from methy ester of conjugated linoleic acid by the reaction of CLA methyl ester with SeO

. The products were purified by semi-normalphase highperformance liquid chromatography and their chemical structures were characterized by liquid chromatography mass spectrometry (LC-MS) and nuclear magnetic resonance spectroscopy (NMR).

关键词

共轭亚油酸双羟基衍生物反应机制谱学特征

Keywords

conjugated linoleic aciddi-hydroxylated derivativesreaction mechanismcharacterization

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